TRIS(4-ETHOXYPHENYL)BISMUTH CAS#: 90591-48-3; 凯望编码 (ChemWhat Code): 1296140

IdentificationPhysical DataSpectra
Route of Synthesis (ROS)Safety and HazardsOther Data

Identification

英文名TRIS(4-ETHOXYPHENYL)BISMUTH
IUPAC Nametris(4-ethoxyphenyl)bismuthane
分子结构TRIS4-ETHOXYPHENYLBISMUTH-CAS-90591-48-3
CAS编号 90591-48-3
别名TEPB, tris-(4-ethoxy-phenyl)-bismuthine, tri(p-ethoxyphenyl)bismuth, Tris-(4-aethoxy-phenyl)-bismutin, Tris-(4-aethoxy-phenyl)-wismut
分子式C24H27BiO3
分子量572.457
InChIInChI=1S/3C8H9O.Bi/c3*1-2-9-8-6-4-3-5-7-8;/h3*4-7H,2H2,1H3;
InChI KeyPBBDAZHUSYNCOV-UHFFFAOYSA-N
Canonical SMILESCCOC1=CC=C(C=C1)[Bi](C2=CC=C(C=C2)OCC)C3=CC=C(C=C3)OCC
Patent Information
Patent IDTitlePublication Date
US2015/112104Process For Producing Chlorinated Hydrocarbons In The Presence Of A Polyvalent Bismuth Compound2015
EP2133357LIVING RADICAL POLYMERIZATION PROMOTER2009
US2006/148842Nepetalactams and N-substituted derivatives thereof2006
US4225517Process for the production of acetaldehyde by the reaction of methanol with synthesis gas1980
US4364872Method of making aluminum alkyls1982

Physical Data

AppearanceWhite or off-white crystal
Melting Point, °C Solvent (Melting Point)
73
87 – 88methanol
86 – 87

Spectra

Nucleus (NMR Spectroscopy)Solvents (NMR Spectroscopy)
1Hdimethylsulfoxide-d6
TRIS(4-ETHOXYPHENYL)BISMUTH CAS#: 90591-48-3 HNMRTRIS(4-ETHOXYPHENYL)BISMUTH CAS 90591-48-3 HNMR
TRIS(4-ETHOXYPHENYL)BISMUTH CAS#: 90591-48-3 HPLC TRIS(4-ETHOXYPHENYL)BISMUTH CAS 90591-48-3 HPLC

Route of Synthesis (ROS)

Route of Synthesis (ROS) of TRIS(4-ETHOXYPHENYL)BISMUTH CAS 90591-48-3
ConditionsYield
Stage #1: bromobenzene With magnesium In tetrahydrofuran Inert atmosphere; Reflux;
Stage #2: bismuth(III) chloride In tetrahydrofuran at -10 – 65℃; for 1.5h; Inert atmosphere; 		51.8%

Safety and Hazards

Pictogram(s)exclamation-mark
SignalDanger
GHS Hazard StatementsH302: Harmful if swallowed [Warning Acute toxicity, oral]
H312: Harmful in contact with skin [Warning Acute toxicity, dermal]
H332: Harmful if inhaled [Warning Acute toxicity, inhalation]
Information may vary between notifications depending on impurities, additives, and other factors. 
Precautionary Statement CodesP261, P264, P270, P271, P280, P301+P312, P302+P352, P304+P312, P304+P340, P312, P322, P330, P363, and P501
(The corresponding statement to each P-code can be found at the GHS Classification page.)

Other Data

TransportationNot dangerouse goods
Under the room temperature and away from light
HS Code294200
StorageUnder the room temperature and away from light
Shelf Life2 years
Market PriceUSD 1500/kg
Use Pattern
TRIS(4-ETHOXYPHENYL)BISMUTH CAS#: 90591-48-3 is added to the fuel of rocket as cruing agent.

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